Item Of Analysis
|
IP/BP Limit
|
USP Limit
|
Results
|
Description
|
Colorless crystals or a white crystalline powder, Odorless,
|
Colorless crystals, Odorless,
|
White crystalline powder
|
Identification
|
a)It gives the reactions of Potassium salts.
b)It gives the reactions of Chlorides
|
a)It gives the reactions of Potassium salts.
b)It gives the reactions of Chlorides
|
Complies
|
Appearance of solution
|
Solution A is clear and colorless.
|
Solution A is clear and colorless.
|
Complies
|
Solubility (solution 10% in water)
|
Freely soluble in water and practically insoluble in ethanol and in ether.
|
Freely soluble in water
|
Complies
|
Acidity/ Alkalinity
|
Not more than 0.5 ml of 0.01 M NaOH or 0.01M Hydrochloric acid is required for neutralization of Bromothymol blue solution.
|
Passes test
|
Complies
|
Arsenic
|
Not more than 1 ppm.
|
|
Complies
|
Heavy Metals
|
< 10 ppm
|
|
Complies
|
Calcium and Magnesium
|
The solution remains clear.
|
No turbidity is produced within 5 mins.
|
Complies
|
Bromides
|
NMT 0.1%
|
NMT 0.1%
|
Complies
|
Sodium
|
NMT 0.1%
|
Passes test
|
0.0848%
|
Iodides
|
No blue colour is observed after 5 mins.
|
NMT 0.005 %
|
Complies
|
Sulphates
|
Less than 300 ppm.
|
|
Complies
|
Barium
|
Solution remains clear
|
|
Complies
|
Iron
|
NMT 20 ppm.
|
|
Complies
|
Loss on drying
|
1.0 % max at 105 deg C for 2 hrs
|
NMT 1.0 % max at 105 deg C for 2 hrs
|
0.49% (when packed)
|
Assay
|
NLT 99.0 and NMT 100.05% on dried basis
|
99.0 TO 100.05%
|
99.76%
|